SALD-2300
Catalog/Part Number:: SALD-2300
Description
Using the SALD-MS23 sampler, the measurement range is 17nm to 2500μm for wet measurement.
For example, PSL particles with a median diameter of 50nm and stainless balls with a diameter of 2mm can be measured by a single analyzer.
By enabling measurement under wide particle concentration conditions (0.1ppm to 20%), changes in particle size distribution depending on particle concentration can be evaluated.
Previously, the particle concentration of a sample had to be adjusted to meet the optimum conditions of analyzers by dilution or concentration using a centrifuge. In these cases, changes in particle size distribution, such as agglomerations or dispersions, could not be considered.
Dispersions and agglomeration can be caused by dilutions.
In some cases, dilutions can accelerate dispersions, but in other cases, they can create agglomerates. To ensure optimum, the initial particle concentration must be determined without dilutions or concentrations. After the evaluation of particle size distribution at the initial state, the effects of particle concentration from dispersions and agglomerations must be evaluated.
Wide particle concentration range must be covered to evaluate the dissolution process of sample particles.
This is necessary because the progress of dissolution makes the particle concentration low in comparison to the first particle concentration.
SALD-2300 can measure particle size distribution under the conditions of particle concentration from 0.1ppm to 20%.
When the sampler SALD-MS23 or batch cell SALD-BC23 is used, measurements are possible under conditions of concentration from 0.1ppm to 100ppm.
When the high-concentration sample measurement system SALD-HC23 is used, high-concentration samples up to 20% can be measured because the negative effects of multiple scattering are prevented.
Technical Specifications
|
Measurement principle |
Laser Diffraction Method |
|
Measurement
range |
SALD-MS23: 17nm(0.017μm) to 2500μm |
|
SALD-BC23: 17nm(0.017μm) to 400μm |
|
|
SALD-HC23: 30nm(0.030μm) to 280μm |
|
|
SALD-DS5: 300nm(0.3μm) to 2500μm |
Note 1: The measurement range varies according to the shape
etc. of the particle.
Measurement Unit: SALD-2300 (P/N: 347-61700-42[115V],
347-61700-44[230V])
|
Light source |
Red Semiconductor laser (Wavelength 680 nm) |
|
Light
detector |
Detector elements for UV semiconductor laser |
|
System
Compliance |
Class 1 Laser Product, CE compliant |
|
Required
power supply |
115 or 230 VAC as ordered 100 VA |
|
Dimensions
& weight |
W680mm×D280mm×H430mm, 31kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
Note 2: Reference sample and USB cable (2 m) supplied as
standard
Sampler: SALD-MS23 (P/N: 347-61701-42[115V],
347-61701-44[230V])
|
Dispersing bath |
Capacity: 100~280cm3 |
|
Sonicator |
Frequency about 32 kHz, output about 40 W |
|
Liquid
Pump |
Radial pump, maximum flow rate 2000cm3/min |
|
Liquid
Pump Material |
Stainless (SUS 304, SUS 316), Tetrafluoroethylene (PTFE),
Perfluoroelastmor (FEP) or Kalrez, Thermoflon Pascal (inside) |
|
Liquid
Supply Pump |
Diaphragm pump, maximum flow rate 750cm3/min |
|
Liquid
Supply Pump Material |
Tetrafluoroethylene, polyvinyl dene fluoride |
|
Flow
Cell |
Quartz glass |
|
Required
power supply |
115 or 230 VAC as ordered, 200 VA |
|
Dimensions
& weight |
W390mm×D520mm×H430mm,18kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
Note 3: USB cable (2 m) supplied as standard
Batch Cell: SALD-BC23 (P/N: 347-61702-42)
|
Cell Material |
Quartz glass |
|
Required
Liquid Volume |
Approx. 12 cm3 |
|
Stirrer
Mechanism |
Up-and-down movement of blade |
|
Dimensions
& weight |
W100mm×D120mm×H140mm, 0.8kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
High-concentration Sample Measurement System: SALD-HC23
(P/N: 347-61703-42)
|
Cell Material |
Borosilicate glass |
|
Required
Liquid Volume |
Approx. 0.15 cm3 |
|
Dimensions
& weight |
W20mm×D100mm×H9mm, 0.2kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
Cyclone Injection Type Dry Measurement Unit: SALD-DS5
(P/N: 347-61706-42[115V], 347-61706-44[230V])
|
Sample suction types |
Cyclone type / One shot type / Hand shot type |
|
Suction
nozzle |
Can be selected from 3 types |
|
Sampling
Unit Specifications |
|
|
System |
Cyclone type |
|
Communication
method |
USB (PC control) |
|
Required
power supply |
115/230VAC(±10%), 100VA, 50/60Hz (excluding dust collector
and compressor) |
|
Dimensions
& weight |
W 240×D 310×H 210 mm, 10 kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
|
Pressure
Regulator Specifications |
|
|
Primary
pressure |
0.6 to 0.8 MPa |
|
Secondary
pressure |
0.05 to 0.5 MPa |
|
Filtration
rating |
Removing particles of 5 μm or larger |
|
Connection
to air source |
Tube of 6 mm outside diameter |
|
Communication
method |
USB (PC control) |
|
Required
power supply |
115/230VAC(±10%), 100VA, 50/60Hz (excluding dust collector
and compressor) |
|
Dimensions
& weight |
W 130×D 223×H 233 mm, 3 kg |
|
Operating
Environment |
Temperature: 10 to 30°C, Humidity: 20 to 80 % (no
condensation) |
Requirements for compressor and dust collector
|
Compressor |
Output |
0.4 kW |
|
|
Minimum pressure |
Approx. 7 kgf/cm2 (approx. 0.69 MPa) |
|
Air discharge |
45 L/min |
|
|
Tank volume |
Approx. 30 L |
|
|
Dust
collector |
Type |
Vacuum cleaner (Paper pack type) |
|
Dust collecting efficiency |
More than 99% for 0.3 μm particles |
|
|
Capacity |
2.0 m3/min or more |
|
|
Vacuum |
Approx. 2000 mm Aq or lower |
|
|
Suction hose diameter |
Approx. 32 mm |
Software
Specifications
WingSALD II
|
Measurement and Data Display Functions |
|
|
Measurement
of Particle Size Distribution |
Allows measurements using measurement assistant function
(interactive process based on SOP) |
|
Refractive
Index Setting |
Automatic refractive index calculation function (LDR method:
Light Intensity Distribution Reproduction Method) makes setting the
refractive index easy. |
|
Real-Time
Display |
Particle size distribution/light intensity distribution
simultaneous display |
|
Diagnostics/Adjustments |
Self-diagnostic function and cell check function |
|
Recalculation
of Particle Size Distribution |
Batch recalculation of max. 200 distributions |
|
Display
of Particle Size Distribution Data |
Displays overlay of max. 200 distributions |
|
Display
of Light Intensity Distribution |
Displays overlay of max. 200 distributions |
|
Statistical
Data Processing |
Max. 200 sets of data (also allows overlaying max. 200
data sets) |
|
Time-Series
Processing |
Max. 200 sets of data |
|
3-Dimensional
Graphing |
Max. 200 sets of data |
|
Data
Transfer via Clipboard |
[Image Output]: Outputs entire data sheet or graph only. |
|
Data
Sorting |
Sorts by file name, sample ID, sample number, or
refractive index |
|
Output
Conditions |
|
|
Particle
Size (μm) Divisions |
Fixed 51 or 101 divisions : User
settable 51 divisions |
|
Particle
Amount (%) Divisions |
Fixed 51 divisions : User settable 51 divisions |
|
Distribution
Basis |
Count, length, area, or volume |
|
Expression
of Cumulative Distribution |
Oversized or undersized |
|
Expression
of Frequency Distribution |
q, q / Δ×, q / Δlog × |
|
Smoothing
Levels |
10 levels |
|
Distribution
Function Fitting |
Rosin-Rammler distribution, logarithmic Gaussian
distribution |
|
Data
Shifting |
±10 levels |
|
Report
Function |
Single data sets (6 templates), overlaid data (5
templates), statistical data, time-series data, or 3D data can be selected
and output using batch processing |
|
Data
Analysis Functions |
|
|
Scattering
Angle Evaluation Function |
Evaluates scattering characteristics within micro angle
regions for samples such as optical films and sheets. |
|
Data
Emulation Functions |
Emulates measurement results from other instruments and
measurement principles, using SALD series measurement results. |
|
Mixture
Data Simulation Function |
Simulates particle size distributions using any mixture
ratio of multiple particle size distributions. |
|
Data
Connection Function |
Combines two particle size distributions with different
measurement ranges at any particle size point to create a single particle
size distribution. |
|
Continuous
Measurement Function |
Continuously measures changes in particle size
distributions and particle diameters over time, at intervals as short as one
second, and saves the results. |
Note 4:The LDR method automatically calculates an
appropriate refractive index based on consistency between the actual measured
light intensity distribution and one reproduced (recalculated) from particle
size distribution data. This method was developed by Shimadzu and published in
two technical papers. It is sometimes called the "Kinoshita Method",
in academic communities, after the name of Shimadzu’s engineer.
PC Requirements
The software is included standard on a CD-R with the SALD
system (optical system).
Install the software on a PC that meets the following specifications.
|
OS |
Windows
7 |
|
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